Characterization of titanium powders processed in n-hexane by high-energy ball milling

A. H. Restrepo, J. M. Ríos, F. Arango, E. Correa, A. A. Zuleta, A. Valencia-Escobar, F. J. Bolivar, J. G. Castaño, F. E. Echeverría

Resultado de la investigación: Contribución a una revistaArtículo

Resumen

The effect of speed and milling time on the morphology, crystallite size, and phase composition of Ti Cp powders processed in n-hexane by high-energy ball milling (HEBM) using a E-max Retsch equipment was studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and transmission electron microscopy (TEM). Lattice parameters, mean crystallite size, lattice strain, and dislocation density were obtained from Rietveld analysis. The XRD and TEM results show that the HEBM process of the Ti Cp promotes the transition from HCP to FCC after 6 h of milling at 1400 rpm. The transformation process could be attributed to the energy generated in the milling process which induces high deformation and presence of high-density dislocations in the powder. Graphical Abstract[Figure not available: see fulltext.].

Idioma originalInglés
Páginas (desde-hasta)1681-1690
Número de páginas10
PublicaciónInternational Journal of Advanced Manufacturing Technology
Volumen110
N.º7-8
DOI
EstadoAceptada/en prensa - 2020

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    Restrepo, A. H., Ríos, J. M., Arango, F., Correa, E., Zuleta, A. A., Valencia-Escobar, A., Bolivar, F. J., Castaño, J. G., & Echeverría, F. E. (Aceptado/En prensa). Characterization of titanium powders processed in n-hexane by high-energy ball milling. International Journal of Advanced Manufacturing Technology, 110(7-8), 1681-1690. https://doi.org/10.1007/s00170-020-05991-7